DEVELOPMENT OF BI-FUNCTIONAL HETEROGENEOUS CATALYST FOR THE PRODUCTION OF BIODIESEL FROM SHEA NUT OIL
Abstract
This study investigates the development and characterization of a bifunctional
heterogeneous catalyst for biodiesel production using calcined oyster shells, alumina, and
plantain peel ash as precursor materials. The oyster shells provided a calcium oxide
(CaO) base source. The catalysts were synthesized via co-precipitation and thermal
calcination at optimized conditions, ensuring the formation of active sites for both
esterification and transesterification reactions. Characterization techniques, including Xray diffraction (XRD),and Brunauer–Emmett–Teller (BET) surface area analysis, were
employed to evaluate the structural, morphological, and surface properties of the
catalyst.The synthesized catalyst demonstrated high catalytic efficiency In biodiesel
production from Shea nut oil under mild reaction conditions, achieving a conversion
yield of over 90%. Its bifunctional properties allowed effective conversion of both free
fatty acids and triglycerides, minimizing pre-treatment steps. Reusability tests confirmed
the catalyst’s stability, retaining activity over four reaction cycles.
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